TITLE: Fast detection of triacetone triperoxide (TATP) from headspace using planar solid-phase microextraction (PSPME) coupled to an IMS detector
AUTHORS: Fan, Young, Canino, Smith, Oxley and Almirall - Florida International University, USA
INSTRUMENT: FloVac
USAGE: After degassing, nitrogen BET was performed on the samples
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TITLE: Formulation and delivery of improved amorphous fenofibrate solid dispersions prepared by thin film freezing
AUTHORS: Meimei Zhang, Houli Li, Bo Lang et al - Sun Yat-sen University, China
INSTRUMENT: Thermoflow
USAGE: Powder samples were placed into the sample bulb, degassed for a minimum of 24 hours at 30˚С prior to analysis
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TITLE: Measuring surface area of airborne titanium dioxide powder agglomerates: relationships between gas adsorption, diffusion and mobility-based methods
AUTHORS: LeBouf, Ki Ku, Chen, Frazer, Cumpston, Stefaniak - National Institute for Occupational Safety and Health, USA
INSTRUMENT: FloVac
USAGE: Blank and particle-laden filter samples were degassed under light vacuum (1.9 Pa) at 120 °C for 24 h prior to analysis.
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TITLE: Influence of the alkoxide group, solvent, catalyst, and concentration on the gelation and porosity of hexylene-bridged polysilsesquioxanes
AUTHORS: Loy, Obrey-DeFriend, Wilson Jr et al - University of Arizona, USA
INSTRUMENT: Quantachrome Degasser
USAGE: Prior to surface area analysis, samples were outgassed on a Quantachrome six port degasser for 18 h at 100 °C
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TITLE: Kinetics study and crystallization process design for scale‐up of UiO‐66‐NH2 synthesis
AUTHORS: Schoenecker, Belancik, Grabicka, Walton - Georgia Institute of Technology, USA
INSTRUMENT: FloVac
USAGE: Prior to each adsorption measurement, the sample was outgassed for approximately 16 h at 473 K
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TITLE: Is their potential for post-synthetic brominating reactions on benzene bridged PMOs?
AUTHORS: Smeulders, Meynen,Houthoofd, Mullens, Martens, Maes, Cool - University of Antwerpen, Belgium
INSTRUMENT: Autosorb Degasser
USAGE: Prior to N2-sorption, all samples were outgassed at 363 K for 16 h.
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TITLE: Rates of Exchange of Cs+ and Sr2+ for Poorly Crystalline Sodium Titanium Silicate (CST) in Nuclear Waste Systems
AUTHORS: Clearfield, Medvedeva, Kerlegona, Bossera, Burnsa & Jackson - Texas A&M University, USA
INSTRUMENT: Quantachrome degasser
USAGE: The samples (0.2-0.6 g) were preheated at temperatures of 225–300°C for 12 h … at the pressure of 2 × 10−3 Torr.
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TITLE: Mesoporous titania photocatalyst: effect of relative humidity and aging on the preparation of mesoporous titania and on its photocatalytic activity performance
AUTHORS: Ibrahim, Masrom, Mazinani, Radiman, Jamil, Beitollahi, Negishi and Yahya - Advanced Material Research Centre (AMREC), Malaysia
INSTRUMENT: Autosorb-1
USAGE: After degassing of the sample at 150 °C for 6 h, the surface area was measured by use of nitrogen absorption–desorption (BET)
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TITLE: Testing of Brushite (CaHPO4·2H2O) in Synthetic Biomineralization Solutions and In Situ Crystallization of Brushite Micro-Granules
AUTHORS: Miller, Kendall, Jain, Larson, Madden and Tas - University of Oklahoma, USA
INSTRUMENT: Nova 2000e
USAGE: Surface areas of powder samples were determined by five-point BET analysis of the nitrogen adsorption isotherm, obtained at −196°C after degassing overnight at 30°C
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TITLE: Material Characterization and Bioactivity Evaluation of Dental Porcelain modified by Bioactive Glass
AUTHORS: Manda, Goudouri, Papadopoulou, Kantiranis et al - Aristotle University of Thessaloniki, Greece
INSTRUMENT: Autosorb-1MP
USAGE: Textural characterization was performed by Nitrogen (N2) adsorption-desorption experiments, after degassing the samples at 320 °C for 16 hours under 5 × 10 −9 torr vacuum
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